N excess of body fat in European adolescents: the HELENA Study. Am J Prev Med 2010, 39:20311. 37. Gracia-Marco L, Moreno LA, Ortega FB, Leon F, Sioen I, Kafatos A, MartinezGomez D, Widhalm K, Castillo MJ, Vicente-Rodriguez G: Levels of physical activity that predict optimal bone mass in adolescents: the HELENA study. Am J Prev Med 2011, 40:59907.doi:10.1186/1741-7015-11-172 Cite this short article as: Jim ez-Pav et al.: Physical activity and clustered cardiovascular disease danger factors in young children: a cross-sectional study (the IDEFICS study). BMC Medicine 2013 11:172.
organic compoundsActa Crystallographica Section EStructure Reports OnlineISSN 1600-= 100.867 (two) V = 1551.37 (11) A3 Z=4 Mo K radiation= 2.66 mm T = 200 K 0.35 0.16 0.07 mmData collection2-(4-Bromophenyl)-2-oxoethyl naphthalene-1-carboxylateBhadrachari Garudachari,a Arun M. Isloor,a Thomas Gerber,b Eric Hostenb and Richard Betzb*aBruker APEXII CCD diffractometer Absorption correction: multi-scan (SADABS; Bruker, 2010) Tmin = 0.656, Tmax = 0.14937 measured reflections 3848 independent reflections 2712 reflections with I two(I) Rint = 0.RefinementR[F 2 two(F 2)] = 0.034 wR(F 2) = 0.080 S = 1.02 3848 reflections 208 parameters H-atom parameters constrained ax = 0.55 e A in = .56 e ANational Institute of Technology-Karnataka, Division of Chemistry, Surathkal, Mangalore 575 025, India, and bNelson Mandela Metropolitan University, Summerstrand Campus, Department of Chemistry, University Way, Summerstrand, PO Box 77000, Port Elizabeth, 6031, South Africa Correspondence e-mail: [email protected] Received 26 February 2013; accepted 27 March 2013 Important indicators: single-crystal X-ray study; T = 200 K; mean (C ) = 0.003 A; R aspect = 0.034; wR aspect = 0.080; data-to-parameter ratio = 18.5.TableHydrogen-bond geometry (A, ).D–H C12–H12 1 C23–H23 3iiiD–H 0.95 0.H 2.41 two.D 3.240 (3) three.292 (three)D–H 146Symmetry codes: (i) 1; ; ; (ii) 1; y 1; 1. 2In the title compound, C19H13BrO3, an ester of 1-naphthoic acid with an aromatic alcohol, the least-squares planes defined by the C atoms of your respective aromatic systems enclose an angle of 77.Ajudecunoid A 20 (5) .Bosentan Inside the crystal, C–H contacts connect the molecules into undulating sheets parallel (100).PMID:23773119 Data collection: APEX2 (Bruker, 2010); cell refinement: SAINT (Bruker, 2010); data reduction: SAINT; system(s) applied to solve structure: SHELXS97 (Sheldrick, 2008); plan(s) made use of to refine structure: SHELXL97 (Sheldrick, 2008); molecular graphics: ORTEP-3 for Windows (Farrugia, 2012); computer software utilized to prepare material for publication: SHELXL97 and PLATON (Spek, 2009).Associated literatureFor basic information about phenacyl bromide derivatives, see: Rather Reid (1919). For the photolytic properties of phenyl benzoates, see: Sheehan Umezaw (1973); Ruzicka et al. (2002); Litera et al. (2006). For synthetic applications of phenyl benzoates, see: Huang et al. (1996); Gandhi et al. (1995). For graph-set analysis of hydrogen bonds, see: Etter et al. (1990); Bernstein et al. (1995). AMI thanks Professor Swapan Bhattacharya, Director of your National Institute of Technology Karnataka, Surathkal, India, for his encouragement and supplying the study facilities. AMI also thanks the Department of Atomic Power, Board for Study in Nuclear Sciences, Government of India for the ‘Young Scientist’ award.Supplementary data and figures for this paper are readily available from the IUCr electronic archives (Reference: QK2054).
Izak-Nau et al. Partic.
